Ion exchange column for removal of hardness of water

Materials & Reagents Required:

  1. Tap water (100 mL)
  2. Conical flask (250 mL)
  3. Weighing balance
  4. Dropper
  5. Glass column
  6. Measuring cylinder (10 mL)
  7. Burette (50 mL)
  8. Cation exchange resin
  9. EDTA (0.01 M)
  10. Ammonia buffer (pH 10)
  11. EBT indicator

    Laboratory Procedure




    Repeat Step-5 and Step-6 three times.

    Procedure in laboratory


    Observation

    The color of soft water instantly changes into blue, while the hard tap water turns wine red when Eriochrome black T is added. The wine-red colored solution turns blue when titrated against the EDTA solution

    Formula: Total hardness of water mg/L = ml of EDTA used unboiled x 103 / ml of sample